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What goes wrong

It caked

On this page10
A dry supplement that has set solid is unusable rather than imperfect.

Caking

The product takes up moisture and sets. It is the defining failure of the dry half of this category, and it happens in storage rather than in production.

Where the moisture comes in

An inadequate seal, a liner that did not land properly, dust on the sealing surface at filling, or a customer opening and reclosing the container in a humid building.

Dust at the fill is the one you control

Filling a dry product at speed throws dust, and dust between a liner and a rim is a seal that looks closed and is not. Wiping the rim belongs in the process rather than in the instructions.

Settling, which is not caking

The product compacts in transit and the container looks underfilled. Nothing is wrong, and customers report it as if something is, which is an argument for declaring by weight and saying so clearly.

Separation in a blend

Ingredients of different particle sizes separate when a container is shaken and carried. A premix that was homogeneous at packing can deliver a different dose from the top than the bottom.

Which is a real compliance exposure

A guaranteed analysis is a statement about the product in the container. If it segregates, a sample taken from the top may not meet the guarantee even though the batch did.

Test it the way it lives

Filled, closed, warm, humid, for weeks, then shaken and opened. Weigh it, look at the liner, and sample from the top and the bottom.

Anti-caking agents are a formulation answer, not a packaging one

They work, they are declared on the ingredient list like anything else, and they do not substitute for a seal. A product that needs both should have both rather than one standing in for the other.

Tell the customer how to store it

Cool, dry, closed, and not on a concrete floor. It costs a line on the label and it prevents the failure that generates the most complaints in this category.

References

The Davis Pack Supply catalog, measured 18 October 2026. The animal and apiary shelf is 854 rows: 399 containers and 455 closures, derived from two archetypes across four leaves. 224 PET, 100 HDPE, 74 glass and 1 LDPE, from 10 to 9,464 mL with a median of 118 and 22 containers at a litre or more. The closures include 43 dropper assemblies, 20 dome lids and 16 flip tops.
21 CFR 501.4, animal food ingredient declaration. Ingredients "shall be listed by common or usual name in descending order of predominance by weight", with specific rather than generic names and limited exceptions; 501.110 permits certain collective names in livestock and poultry feeds. law.cornell.edu
Written from 21 CFR 501.4, 507.5 and 589.2000, and from the catalog as it stood on 18 October 2026. Commercial feed is also registered and labeled under state law, which this property points at rather than covers; whether a given product is a feed, a supplement or a drug is a determination with consequences, and a medicated feed is a different regime again.